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Validasi Metode dan Penetapan Kadar Residu Furazolidon dalam Udang secara Kromatografi Cair Kinerja Tinggi

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Title Validasi Metode dan Penetapan Kadar Residu Furazolidon dalam Udang secara Kromatografi Cair Kinerja Tinggi
 
Creator Soedjito, Soedjito
Azminah, Azminah
Soediman, Soediatmoko
 
Subject RS Pharmacy and materia medica
 
Description Furazolidon is one of antibacterial nitrofuran derivate used in prawn cultivation. Existence of residue furazolidon in prawn can cause the carcinogenic effect, toxic effect, allergic reaction, and also improve the resistancy when it is consumed in along term. In this research were done validating method and determining of concentration of furazolidon residue in a various type of prawn used the High Performance Liquid Chromatography (HPLC) with the column of Phenomenex type Hypersil 5 µ m C18 (ODS) 25 cm, Φ 4.60 mm, loop 500 µl, detector UV λ at 366 nm, asetonitril : acetic acid 1% = 20-100 : 80-0 as mobile phase during 8 minutes, flow-rate 1.0 mL/minute, temperature 30.3 oC, pressured 3.6 – 9.8 psi. The results of the validation method analyze were met the validation criterion i.e., selectivity, linearity, accuracy, precision, LOD and LOQ. The residues concentration of furazolidon in prawn samples of Penaeus vanamei from Market A were 8.56x10-3 mg/100 g, while the residues of furazolidon in samples of prawn of Penaeus vanamei from Market of B, Metapenaeus monoceros from Market C, and Penaeus monodon from Market D were not found.
 
Publisher Lembaga Penelitian dan Pengabdian Kepada Masyarakat, Universitas Surabaya
 
Date 2007-02
 
Type Article
PeerReviewed
 
Format application/pdf
 
Language en
 
Identifier /232/1/Azminah_Validasi%20Metode%20dan%20Penetapan%20Kadar%20Residu_Abstrak_2007.pdf
Soedjito, Soedjito and Azminah, Azminah and Soediman, Soediatmoko (2007) Validasi Metode dan Penetapan Kadar Residu Furazolidon dalam Udang secara Kromatografi Cair Kinerja Tinggi. Jurnal Ilmiah Sains & Teknologi, 2 (2). pp. 113-127. ISSN 0216-1540